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Structure and electrochemical properties of FeSx nanoparticles synthesized by chemical vapor condensation process

Authors
Ha, Jong-KeunCho, Kwon-KooKim, Ki-WonKim, Jong-UkKim, Yoo-Young
Issue Date
2006
Publisher
TRANS TECH PUBLICATIONS LTD
Keywords
metal sulfide; chemical vapor condensation (CVC) process; nanoparticles; FeSx electrode
Citation
ECO-MATERIALS PROCESSING & DESIGN VII, v.510-511, pp 950 - 953
Pages
4
Indexed
SCIE
SCOPUS
Journal Title
ECO-MATERIALS PROCESSING & DESIGN VII
Volume
510-511
Start Page
950
End Page
953
URI
https://scholarworks.gnu.ac.kr/handle/sw.gnu/29155
DOI
10.4028/www.scientific.net/MSF.510-511.950
ISSN
0255-5476
1662-9752
Abstract
FeSx nanoparticles were synthesized by the chemical vapor condensation (CVC) process using the pyrolysis of iron pentacarbonyl (Fe(CO)5) and sulfur (S). The influence of CVC parameter on the formation of nanoparticle and size distribution was studied. The synthesized nanoparticles consisting of FeS, FeS2 and Fe2O3 were nearly spherical shape and 5 similar to 40 nm in mean diameter. Obtained particles were studied by applying the field emission scanning electron microscopy (FESEM) and high resolution transmission electron microscopy (HRTEM) and X-ray diffraction (XRD) methods. Electrochemical properties of the electrode fabricated with synthesized nanoparticles were evaluated.
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우주항공대학 (항공우주공학부)
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