Tandem One-Pot Synthesis of 2 <i>H</i> - and 3 <i>H</i> -Pyrroles Enabled by Dual Rh(II)/Pd(0) Catalysis
  • Choi, Seoung-Mi
  • Yun, Yuri
  • Kim, Ju Hyun
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초록

Regioselective approaches toward 2H- and 3H-pyrroles,which are biologically important but easily isomerizable compounds, have been successfully achieved via dual Rh(II)/Pd(0) relay catalysis and DBU-mediated processes in one-pot operation using N-tosyltriazoles and hydroxymethylallyl carbonates. In this transformation, readily accessible N-tosyltriazoles were enabled as stable nitrogen sources for the two scaffolds, and the regioselectivity was controlled by the substituent positions of the hydroxymethylallyl carbonates.

키워드

2H -pyrrole3H -pyrroledual catalysisregioselectivityN -tosyltriazoleASYMMETRIC ALLYLIC DEAROMATIZATIONENANTIOSELECTIVE SYNTHESISFUNCTIONALIZATIONHETEROCYCLESCASCADEESTERSSPIRO
제목
Tandem One-Pot Synthesis of 2 <i>H</i> - and 3 <i>H</i> -Pyrroles Enabled by Dual Rh(II)/Pd(0) Catalysis
저자
Choi, Seoung-MiYun, YuriKim, Ju Hyun
DOI
10.1055/a-2312-5815
발행일
2024-11
유형
Article
저널명
Synthesis
56
22
페이지
3405 ~ 3411