Synthesis of a small molecular cage consisting of three aminomethyl pyrroles and its selective fluoride recognition
Synthesis of a small molecular cage consisting of three aminomethyl pyrroles and its selective fluoride recognition
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초록

A small cage-like molecule (2) composed of three aminomethyl pyrroles and two hexa-substituted benzenes has been prepared by reduction of its iminopyrrole analogue (1) using NaBH4. It was revealed by 1H NMR spectroscopic analyses that cage molecule 2 strongly binds the fluoride anion in polar DMSO-d6 relative to CDCl3. Compared to that of compound 1, the lowered affinity of 2 for the fluoride anion is attributable to its increased electron density resulting from the production of thesecondary amine groups.

키워드

molecular cageanion recognitionfluorideaffinityselectivity
제목
Synthesis of a small molecular cage consisting of three aminomethyl pyrroles and its selective fluoride recognition
제목 (타언어)
Synthesis of a small molecular cage consisting of three aminomethyl pyrroles and its selective fluoride recognition
저자
허남중한혜진최재원김성국
DOI
10.6564/JKMRS.2022.26.4.040
발행일
2022-12
유형
Article
저널명
Journal of the Korean Magnetic Resonance Society
26
4
페이지
40 ~ 45