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벤질알코올과 아세토나이트릴의 반응을 통한 -hydroxynitrile의 전기화학적 합성Electrochemical Synthesis of β-Hydroxynitrile by addition of Acetonitrile into Benzyl Alcohol
- Other Titles
- Electrochemical Synthesis of β-Hydroxynitrile by addition of Acetonitrile into Benzyl Alcohol
- Authors
- Choi, H.; An, J.; Kwon, K.-Y.
- Issue Date
- Aug-2022
- Publisher
- Korean Society of Industrial Engineering Chemistry
- Keywords
- Cyanomethylation; Electrooxidation; Tetrabutylammonium perchlorate; β-hydroxynitrile
- Citation
- Applied Chemistry for Engineering, v.33, no.4, pp 436 - 439
- Pages
- 4
- Indexed
- SCOPUS
ESCI
KCI
- Journal Title
- Applied Chemistry for Engineering
- Volume
- 33
- Number
- 4
- Start Page
- 436
- End Page
- 439
- ISSN
- 1225-0112
1228-4505
- Abstract
- β-Hydroxynitrile and β-ketonitrile were synthesized by the electrochemical oxidation of benzyl alcohol in an acetonitrile solvent. β-Hydroxynitrile was prepared by the reaction between benzaldehyde from the oxidation of benzyl alcohol and acetonitrile anion which was produced from the electrochemical reduction of acetonitrile. β-Hydroxynitrile was finally electrochemically converted into β-ketonitrile by applying 20 mA of current for 3 h. We demonstrated that β-hydroxynitrile or β-ketonitrile syntheses were prepared by electrochemical oxidation of benzyl alcohol with a commonly used Pt electrode at room temperature. ? 2022 The Korean Society of Industrial and Engineering Chemistry. All rights reserved.
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