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Synthesis and Anion Recognition Features of a Molecular Cage Containing Both Hydrogen Bond Donors and Acceptors
- Authors
- Oh, Ju Hyun; Kim, Jeong Hyeon; Kim, Dong Sub; Han, Hye Jin; Lynch, Vincent M.; Sessler, Jonathan L.; Kim, Sung Kuk
- Issue Date
- 7-Jun-2019
- Publisher
- AMER CHEMICAL SOC
- Citation
- ORGANIC LETTERS, v.21, no.11, pp 4336 - 4339
- Pages
- 4
- Indexed
- SCI
SCIE
SCOPUS
- Journal Title
- ORGANIC LETTERS
- Volume
- 21
- Number
- 11
- Start Page
- 4336
- End Page
- 4339
- ISSN
- 1523-7060
1523-7052
- Abstract
- A molecular cage, macrobicycle 2, containing amide and pyrrole groups as hydrogen-bonding donors and imine groups as hydrogen-bonding acceptors has been synthesized. Compound 2 was found to recognize tetrahedral oxyanions with high affinities, such as H2PO4-, HSO4-, SO42-, and HP2O73-, as well as the spherical halide anions, in chloroform. A single-crystal X-ray diffraction analysis revealed that compound 2 formed a 1:1 complex with H2PO4- in the solid state.
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