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Chemoselective synthesis of aryl(pyridinyl)methanol derivatives through Ni-NIXANTPHOS catalyzed alpha-arylation and tandem arylation/rearrangement of pyridylmethyl ethers
- Authors
- 김병선; Liu, ZF (Liu, Zhengfen); Li, MY (Li, Minyan); Wang, BJ (Wang, Bijun); Deng, GG (Deng, Guogang); Chen, W (Chen, Wen); Zhang, HB (Zhang, Hongbin); Yang, XD (Yang, Xiaodong); Walsh, PJ (Walsh, Patrick J.)
- Issue Date
- Jun-2018
- Publisher
- ROYAL SOC CHEMISTRY
- Citation
- ORGANIC CHEMISTRY FRONTIERS, v.5, no.12, pp 1870 - 1876
- Pages
- 7
- Indexed
- SCIE
SCOPUS
- Journal Title
- ORGANIC CHEMISTRY FRONTIERS
- Volume
- 5
- Number
- 12
- Start Page
- 1870
- End Page
- 1876
- ISSN
- 2052-4110
2052-4129
- Abstract
- An efficient synthesis of aryl(pyridyl)-methanol derivatives using a nickel-NIXANTPHOS catalyst is described. Combinations of the Ni-NIXANTPHOS catalyst, solvent, and reaction temperature achieved chemoselective arylation and tandem arylation/rearrangement of pyridylmethyl ethers. A large variety of aryl halides were tolerated (55 examples, up to 96% yield). The scalability of the reaction is demonstrated. The order of the tandem arylation and [1,2]-Wittig rearrangement was probed by comparative studies.
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